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20320-59-6
hoyan
Product description
whatsapp:0086195 6568 0882
rachel@whhoyan.com
Threema id:AAVXFAZX
bmk
The anhydrous ethanol co-vaporized with diethyl phthalate and sodium metal is added dropwise to the mixture of diethyl malonate, carbon tetrachloride and magnesium, heated to start the reaction, and the temperature is controlled to smooth the reaction. Then add anhydrous diethyl ether, heat for 1h, add the diethyl ether solution of phenylacetyl chloride (add slowly, not to make the reaction too intense). After the reaction is completed, cool and add water, separate the oil layer, and evaporate the diethyl ether under reduced pressure to obtain diethyl(phenylacetyl)malonate.
Product Name: | Diethyl(phenylacetyl)malonate |
Synonyms: | Diethyl(phenylacetyl)malonate;Propanedioic acid, 2-(2-phenylacetyl)-, 1,3-diethyl ester;Propanedioic acid, (phenylacetyl)-, diethyl ester;Pharmaceutical intermediates Diethyl(phenylacetyl)malonate;2-(2-phenylacetyl)propanedioate;White Powder New P Pharmaceutical Grade;Diethyl(phenylacetyl)malonate White Powder;White Powder Diethyl(phenylacetyl)malonate |
CAS: | 20320-59-6 |
MF: | C15H18O5 |
MW: | 278.3 |
EINECS: | 205-854-1 |
Product Categories: | 20320-59-6;BMK |
Mol File: | 20320-59-6.mol |
bmk
pmk
Product description
whatsapp:0086195 6568 0882
rachel@whhoyan.com
Threema id:AAVXFAZX
bmk
The anhydrous ethanol co-vaporized with diethyl phthalate and sodium metal is added dropwise to the mixture of diethyl malonate, carbon tetrachloride and magnesium, heated to start the reaction, and the temperature is controlled to smooth the reaction. Then add anhydrous diethyl ether, heat for 1h, add the diethyl ether solution of phenylacetyl chloride (add slowly, not to make the reaction too intense). After the reaction is completed, cool and add water, separate the oil layer, and evaporate the diethyl ether under reduced pressure to obtain diethyl(phenylacetyl)malonate.
Product Name: | Diethyl(phenylacetyl)malonate |
Synonyms: | Diethyl(phenylacetyl)malonate;Propanedioic acid, 2-(2-phenylacetyl)-, 1,3-diethyl ester;Propanedioic acid, (phenylacetyl)-, diethyl ester;Pharmaceutical intermediates Diethyl(phenylacetyl)malonate;2-(2-phenylacetyl)propanedioate;White Powder New P Pharmaceutical Grade;Diethyl(phenylacetyl)malonate White Powder;White Powder Diethyl(phenylacetyl)malonate |
CAS: | 20320-59-6 |
MF: | C15H18O5 |
MW: | 278.3 |
EINECS: | 205-854-1 |
Product Categories: | 20320-59-6;BMK |
Mol File: | 20320-59-6.mol |
bmk
pmk